TY-JOURA2-Capell-BarrachinaAU - Galvão, Julia Arantes AU - Yamatogi, Ricardo Seiti AU - Biondo, Alexander Welker AU - Pinto, José Paes de Almeida Nogueira AU - Silva, José Roberto Marques AU - Carbonari, Caio Antonio AU - Velini, Edivaldo Domingues PY - 2017 DA - 2017/01/22 TI - Multiscreening LC-MS/MS Designed for Ten Pesticide and Six Antimicrobial Residues in Eggs SP - 9718451 VL - 2017 AB - A multiscreening method was experimentally validated for pesticide and antimicrobial residues in spiked eggs at levels of 5, 50, and 500 华府 gL ^一号.残留提取法用丙烯酸和1%甲状腺酸执行提取材料存储于-70摄氏度直至LC-MS/MS24小时内检测和量化农药和杀菌残留物回收实现适当的标准偏差,结果从94.10%(ampa)到9.20%(carbyl)不等,从95.70%(enrofroxacin)到46.20%(sulfathia方法高度精准,考虑到所有农药和杀菌残留物的直性 R 2 > 0.99 量化限值从0.78到6.25 华府 gL ^一号0.78至3.13 华府 gL ^一号抗生素高度关联系数 R > 0.99 )被发现,除西维林时间提取和西维林恢复仍有待改进,但方法显示快速检测农药和杀菌残留SN-0146-9428UR-https://doi.org/101155/2017/9718451DO-10.11557/971845